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N-[2-(6-Methyl-4-oxo-4H-chromen-3-yl)-4-oxothia-zolidin-3-yl]furan-2-carbox-amide N,N-dimethyl-formamide solvate.

N-[2-(6-メチル-4-オキソ-4H-クロメン-3-イル)-4-オキソチアゾリジン-3-イル]フラン-2-カルボキサミドのDMF溶媒和物の結晶構造

other not specified not assessed

Abstract

This crystallographic study reports the structure of a DMF solvate of a compound consisting of a furan-2-carboxamide moiety linked through a distorted envelope-conformation 4-oxothiazolidin-3-yl ring to a 6-methyl-4-oxo-4H-chromen-3-yl group. Intermolecular hydrogen bonding includes both strong N–H···O and weak C–H···O interactions involving the DMF solvent and the heterocyclic components. The carbonyl oxygen of DMF acts as a four-center (trifurcated) hydrogen-bond acceptor engaging the carboxamide, furan, and chromenyl groups simultaneously. Dihedral angles between the planar chromone unit and the furan and thiazolidinyl rings were determined to be 89.4° and 78.5°, respectively.

Bibliographic

Authors
Zhao PL, Zhou ZZ
Journal
Acta Crystallogr Sect E Struct Rep Online
Year
2009 (2009-07-29)
PMID
21583697
DOI
10.1107/S1600536809029572
PMC
PMC2977248

Delivery context

The delivery route is not clearly identifiable from this paper. For hydrogen intake, inhalation is the most efficient route; inhalation, however, carries explosion risk (empirical LFL of 10%; high-concentration devices are not recommended).

Safety notes

The delivery route is not clearly identifiable from this paper. For hydrogen intake, inhalation is the most efficient route; inhalation, however, carries explosion risk (empirical LFL of 10%; high-concentration devices are not recommended).

See also:

Cite as: H2 Papers — PMID 21583697. https://h2-papers.org/en/papers/21583697
Source: PubMed PMID 21583697