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2-(3-{(3R,4R)-4-Methyl-3-[meth-yl(7H-pyrrolo-[2,3-d]pyrimidin-4-yl)amino]-piperidin-1-yl}oxetan-3-yl)aceto-nitrile monohydrate.

ピロロピリミジン系化合物一水和物の結晶構造解析

other not specified not assessed

Abstract

The crystal structure of C18H24N6O monohydrate was determined. The piperidine ring adopts a chair conformation, with an N-C-C-C torsion angle of 39.5° between the cis-oriented substituents. A water-mediated intermolecular hydrogen bond is formed between the pyrrole N-H group and a nitrogen atom of the fused pyrimidine ring. Each water molecule bridges two organic molecules and is disordered across two sites with occupancies of 0.48 and 0.52. Crystal packing analysis reveals zigzag chains composed of alternating organic and water molecules extending parallel to the a axis.

Bibliographic

Authors
Gehringer M, Pfaffenrot E, Keck PR, Schollmeyer D, Laufer SA
Journal
Acta Crystallogr Sect E Struct Rep Online
Year
2014 (2014-04-01)
PMID
24826108
DOI
10.1107/S1600536814004449
PMC
PMC3998552

Delivery context

The delivery route is not clearly identifiable from this paper. For hydrogen intake, inhalation is the most efficient route; inhalation, however, carries explosion risk (empirical LFL of 10%; high-concentration devices are not recommended).

Safety notes

The delivery route is not clearly identifiable from this paper. For hydrogen intake, inhalation is the most efficient route; inhalation, however, carries explosion risk (empirical LFL of 10%; high-concentration devices are not recommended).

See also:

Cite as: H2 Papers — PMID 24826108. https://h2-papers.org/en/papers/24826108
Source: PubMed PMID 24826108