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Crystal structure of tris-[bis-(2,6-diiso-propyl-phen-yl) phosphato-κ]penta-kis-(methanol-κ)europium methanol monosolvate.

トリス[ビス(2,6-ジイソプロピルフェニル)ホスファト]ペンタキス(メタノール)ユーロピウム・メタノール単溶媒和物の結晶構造

other not specified not assessed

Abstract

A mononuclear europium complex was isolated as a minor product from the reaction of europium(III) chloride hydrate with lithium bis(2,6-diisopropylphenyl)phosphate in a 1:3 molar ratio in methanol. X-ray diffraction at 120 K revealed monoclinic (2/m) symmetry, and the compound is isostructural with previously characterized lanthanum, cerium, and neodymium analogs. All three phosphate ligands adopt a terminal κ1-coordination mode around the europium center. Hydroxyl hydrogen atoms participate in a total of six O–H···O hydrogen bonds, comprising four intramolecular and two intermolecular interactions. Photophysical characterization confirmed luminescence with a low quantum yield.

Bibliographic

Authors
Kalugin AE, Lyssenko KA, Minyaev ME, Roitershtein DM, Puntus LN, Varaksina EA, et al.
Journal
Acta Crystallogr E Crystallogr Commun
Year
2019 (2019-12-01)
PMID
31871753
DOI
10.1107/S2056989019015421
PMC
PMC6895930

Delivery context

The delivery route is not clearly identifiable from this paper. For hydrogen intake, inhalation is the most efficient route; inhalation, however, carries explosion risk (empirical LFL of 10%; high-concentration devices are not recommended).

Safety notes

The delivery route is not clearly identifiable from this paper. For hydrogen intake, inhalation is the most efficient route; inhalation, however, carries explosion risk (empirical LFL of 10%; high-concentration devices are not recommended).

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Cite as: H2 Papers — PMID 31871753. https://h2-papers.org/en/papers/31871753
Source: PubMed PMID 31871753